HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(tert-Butylaminosulphonyl)benzeneboronic acid → HCID 25097444, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(tert-Butylaminosulphonyl)benzeneboronic acid | HCID 44119538 | — |
| Reactant | 6'-(3-Bromo-phenyl)-2'-methyl-6-trifluoromethyl-[3,4']bipyridinyl | HCID 67393554 | — |
| Product | HCID 25097444 | HCID 25097444 | — |
Reaction Steps
The title compound was prepared from 6′-(3-bromo-phenyl)-2′-methyl-6-trifluoromethyl-[3,4′]bipyridinyl (example B.12) (0.197 g, 0.5 mmol) and commercially available 3-(tert-butylsulfamoyl)-benzeneboronic acid (0.142 g, 0.55 mmol) according to the general procedure III. Obtained as a white foam (0.245 g, 93%). MS (ISP) 526.7 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08012986B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-e9f377dc02d444afbdf163a8e6736d0f |
| Source note | uspto-grants-2011_09 |