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HRID907021

反应详情

EQUATION

反应方程式

HRID 907021 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Li+].[Li+]
HCID11125

Lithium carbonate

CLi2O3

结构：Cc1c(F)ccc(C#N)c1F
HCID11344119

2,4-Difluoro-3-methylbenzonitrile

C8H5F2N

结构：CC(C)[C@@H]1NCC[C@@]1(O)C1CC1
HCID59273011

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@H]1N(c2ccc(C#N)c(F)c2C)CC[C@]1(C)O
HCID59273061

未命名化合物

PROCEDURE

实验过程

By an operation in the same manner as in Example 1 and using (2S,3S)-2-ethyl-3-methylpyrrolidin-3-ol 0.5 oxalate (220 mg), 2,4-difluoro-3-methylbenzonitrile (290 mg) and lithium carbonate (210 mg), the title compound was obtained as pale-yellow oil (yield: 97.3 mg, yield: 29%).