huagongshe.com
HRID907028

反应详情

EQUATION

反应方程式

HRID 907028 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Li+].[Li+]
HCID11125

Lithium carbonate

CLi2O3

结构：Cc1c(F)ccc(C#N)c1F
HCID11344119

2,4-Difluoro-3-methylbenzonitrile

C8H5F2N

结构：CC(C)[C@@H]1NCC[C@@]1(O)C1CC1
HCID59273011

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@H]1N(c2ccc(C#N)c(F)c2C)CC[C@@]1(O)CC
HCID59273026

未命名化合物

PROCEDURE

实验过程

By an operation in the same manner as in Example 1 and using (2S,3S)-2,3-diethylpyrrolidin-3-ol 0.5 oxalate (200 mg), 2,4-difluoro-3-methylbenzonitrile (279 mg) and lithium carbonate (220 mg), the title compound was obtained as pale-yellow oil (yield: 151 mg, yield: 52%).