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HRID907064

反应详情

EQUATION

反应方程式

HRID 907064 的结构方程式

REACTANTS

反应物

2
结构：Cc1noc(C)c1B(O)O
HCID2734346

3,5-Dimethylisoxazole-4-boronic acid

C5H8BNO3

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](OC(C)=O)CS[C@H]1Oc1ccc(Br)cc1F
HCID67399103

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](OC(C)=O)CS[C@H]1Oc1ccc(-c2c(C)noc2C)cc1F
HCID67400144

未命名化合物

收率 59%

PROCEDURE

实验过程

By carrying out the operation analogously to example 3, starting from 4-bromo-2-fluorophenyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside obtained according to preparation VI, and 3,5-dimethyl-4-isoxazoleboronic acid, the expected compound is obtained in the form of a white solid with a yield of 59%.

WORKUP

后处理

  1. customobtained