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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 907065Generated: November 1, 2026

2-Methylpyridine-4-boronic acid → 2-Chloro-5-(2-methyl-4-pyridinyl)phenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside

https://huagongshe.com/reaction/907065

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Methylpyridine-4-boronic acidHCID 4192664—
Reactant5-bromo-2-chlorophenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranosideHCID 67395633—
Product2-Chloro-5-(2-methyl-4-pyridinyl)phenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranosideHCID 67396603—

Reaction Steps

By carrying out the operation analogously to example 3, starting from 5-bromo-2-chlorophenyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside, obtained according to preparation X, and 2-methyl-4-pyridineboronic acid, the expected product is obtained and is reacted further without additional purification in order to obtain the nonacetylated xyloside.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08013010B2
Source datasetuspto-grants-2011_09
ORD IDord-11394fffa15043b5a738fdf9814aef7c
Source noteuspto-grants-2011_09