1-Methylhomopiperazine → HCID 25020558, compound

Participants

Reaction Steps

The product of step iii) (0.1 g) was dissolved in dichloromethane (10 mL) and 1-methyl-1,4-diazepane (0.062 mL) added. The mixture was stirred at room temperature for 5 minutes then sodium triacetoxyborohydride (0.16 g) was added. The mixture was allowed to stand and the solvent allowed to evaporate. Methanol (5 mL) was added and the solution purified directly by HPLC to give the title compound as a solid (30 mg).

Provenance & Evidence