Formaldehyde → HCID 57551806, compound

Participants

Reaction Steps

The product of Example 67 (0.050 g) and formaldehyde (0.079 mL) were stirred in dichloromethane (10 mL). Sodium triacetoxyborohydride (0.067 g) was then added and the mixture stirred at room temperature for 12 hours. The volatiles were removed under reduced pressure and the residue purified by HPLC to give the title compound as a solid (0.035 g).

Provenance & Evidence