Hexahydro-1,4-diazepine → HCID 57551729, compound

HRID 907301Notes

Reaction equation

HRID 907301 reaction equation
[CH:1]1([NH:4][C:5](=[O:30])[C:6]2[CH:11]=[CH:10][C:9]([CH3:12])=[C:8]([C:13]3[CH:14]=[C:15]4[C:20](=[CH:21][CH:22]=3)[C:19](=[O:23])[N:18]([CH2:24][CH:25]3[CH2:27][CH2:26]3)[CH:17]=[C:16]4[CH:28]=O)[CH:7]=2)[CH2:3][CH2:2]1.[NH:31]1[CH2:37][CH2:36][CH2:35][NH:34][CH2:33][CH2:32]1>>[CH:1]1([NH:4][C:5](=[O:30])[C:6]2[CH:11]=[CH:10][C:9]([CH3:12])=[C:8]([C:13]3[CH:14]=[C:15]4[C:20](=[CH:21][CH:22]=3)[C:19](=[O:23])[N:18]([CH2:24][CH:25]3[CH2:26][CH2:27]3)[CH:17]=[C:16]4[CH2:28][N:31]3[CH2:37][CH2:36][CH2:35][NH:34][CH2:33][CH2:32]3)[CH:7]=2)[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 68163Hexahydro-1,4-diazepineHCID 57551737HCID 57551737, compound

Product 1

HCID 57551729HCID 57551729, compound

Procedure

The title compound was prepared as a solid by the method of Example 59 step iv) using product of Example 59 step iii) and 1,4-diazepane.

Sources & evidence

ORD record
ord-4b684a2655354ac3b991ad8b11e48e18
Source dataset
uspto-grants-2011_09
Patent number
US08012979B2

Reaction notes

Loading…