Acetone → HCID 57551751, compound

Participants

Reaction Steps

The product of Example 83 (50 mg) was dissolved in dichloromethane (10 mL) and acetone (0.037 mL) added. The solution was stirred for 5 minutes then sodium triacetoxyborohydride (63.3 mg) added. The mixture was stirred at room temperature for 16 hours. The volatiles were removed under reduced pressure and the residue purified by HPLC to give the title compound as a solid (45 mg).

Provenance & Evidence