Acetone → HCID 86616105, compound

HRID 907436Notes

Reaction equation

[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[F:9].[CH3:10][C:11]([CH3:13])=O>>[F:9][C:3]1[CH:4]=[C:5]([OH:8])[CH:6]=[CH:7][C:2]=1[N:1]=[C:11]([CH3:13])[CH3:10]

Participants

Reactant 2

HCID 180Acetone

HCID 27359194-Amino-3-fluorophenol

Product 1

HCID 86616105HCID 86616105, compound

Procedure

Using the procedure for Example 13, 4-amino-3-fluoro-phenol Compound 14a was refluxed with acetone to provide 3-fluoro-4-isopropylideneamino-phenol Compound 14b in quantitative yield. MS (ESI) m/z: 168 (M+H+).

Sources & evidence

ORD record: ord-823d82f6ccd84d1d9b9fa7f431b34897
Source dataset: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08013153B2

Reaction notes

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