HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178519070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | 4-Amino-6-chloroisobenzofuran-1(3H)-one | HCID 67261323 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178519070 | HCID 178519070 | — |
Reaction Steps
A mixture of 4-amino-6-chloroisobenzofuran-1(3H)-one (1 g, 5.46 mmol), benzaldehyde (0.72 g, 6.79 mmol) and magnesium sulfate (6 g) in dichloromethane (80 mL) was stirred at reflux overnight. The mixture was evaporated under reduced pressure and the residue was dried in vacuum. A crude product was obtained (740 mg) and used in next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08012976B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-46f7d42cec454db18292c63d602e6479 |
| Source note | uspto-grants-2011_09 |