Hydrochloric Acid → HCID 57740557, compound

Participants

Reaction Steps

First, 16 g of 2-naphthaldehyde was dissolved in 150 mL of THF, and 150 mL of allyl magnesium chloride (a 2.0 M THF solution) was slowly added thereto. The resulting mixture was reacted at a temperature of about 45° C. for 8 hours. After the reaction, the reactant was slowly neutralized in an extreme amount of thin hydrochloric acid solution. Then, the extract was extracted therefrom using diethyl ether and purified through column chromatography (hexane:ethyl acetate=3:1), preparing 10 g of 4-(naphthalen-2yl)hepta-1,6-dien-4-ol monomer (yield: 42%).

Provenance & Evidence