Methylamine ethanol → HCID 178485285, compound

Participants

Reaction Steps

Following the procedure for example 24, the product obtained in Example 26 was treated with methylamine/ethanol instead of ethylamine to give the titled compound. LC/MS: m/z 480(M+H). 1H-NMR (500 MHz, d6-DMSO). δ 2.78 (d, 3H), 5.55 (s, 2H), 7.04 (d, 1H), 7.35 (t, 2H), 7.58-7.62 (m, 2H), 7.75 (dd, 1H), 7.92 (d, 1H), 8.04 (s, 1H), 8.44 (d, 1H), 13.1 (d, 1H).

Provenance & Evidence