HCID 59205673, compound → HCID 59205674, compound

Participants

Reaction Steps

A mixture of 10.3 grams (0.033 mole) of 2-(2,6-dichloro-4-(phenylmethoxy)phenoxy)ethan-1-ol and 0.4 gram (catalyst) of 10% palladium on carbon in 100 mL of ethanol was subjected to hydrogenation conditions (40 PSI) using a Parr hydrogenator. After the theoretical uptake of hydrogen, the reaction mixture was filtered and concentrated under reduced pressure, yielding 7.0 grams of the subject compound as a residue. The NMR spectrum was consistent with the proposed structure.

Provenance & Evidence