HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 908662Generated: November 1, 2026
5-Methoxy-4-nitro-1,3-benzothiazole-2-carboxylic acid → HCID 67392978, compound
https://huagongshe.com/reaction/908662
Participants
| Role | Name | HCID | Charge |
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| Reactant | 5-Methoxy-4-nitro-1,3-benzothiazole-2-carboxylic acid | HCID 45480359 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67392978 | HCID 67392978 | 80% |
Reaction Steps
3 g (11.8 mmol) of 5-methoxy-4-nitro-1,3-benzothiazole-2-carboxylic acid is suspended in 200 ml of dichloromethane and heated at 60° C. for 2 hours. The dichloromethane is evaporated off under reduced pressure. 5-methoxy-4-nitro-1,3-benzothiazole is obtained in the form of a beige powder. (m=2 g; yield=80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08017637B2 |
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| Source dataset | uspto-grants-2011_09 |
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| ORD ID | ord-11d39833ff214477b85cd07583ca0deb |
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| Source note | uspto-grants-2011_09 |
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