HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Methoxybenzenethiol → {[4-Hydroxy-1-(3-methoxy-phenylsulfanyl)-isoquinoline-3-carbonyl]-amino}-acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Methoxybenzenethiol | HCID 84989 | — |
| Edukt | FG-2216 | HCID 6914666 | — |
| Produkt | {[4-Hydroxy-1-(3-methoxy-phenylsulfanyl)-isoquinoline-3-carbonyl]-amino}-acetic acid | HCID 66712952 | — |
Reaktionsschritte
The title compound was prepared from [(1-chloro-4-hydroxy-isoquinoline-3-carbonyl)-amino]-acetic acid (U.S. Pat. No. 6,093,730) and 3-methoxybenzenethiol under conditions analogous to Example D-110. The final product was precipitated from a solution of ethyl acetate using hexanes; MS (−) m/z 385.12 (M−1)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08017625B2 |
| Quelldatensatz | uspto-grants-2011_09 |
| ORD ID | ord-d845357a9caf42d2a511c73854cc5bf7 |
| Quellennotiz | uspto-grants-2011_09 |