HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 23150783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Iodine | HCID 807 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 23150766 | HCID 23150766 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23150783 | HCID 23150783 | 193.6% |
Reaction Steps
Following the procedure described in example 7§C, but starting from trans-2,3-dihydro-6-[3-(3-hydroxypropoxy)prop-1-en-1-yl]benzo[1,4]dioxine (280 mg), triphenylphosphine (455 mg), imidazole (114 mg) and diiodine (355 mg) in toluene (2.6 mL) affords 780 mg of trans-2,3-dihydro-6-[3-(3-iodopropoxy)prop-1-en-1-yl]benzo[1,4]dioxine as a clear oil used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017646B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-1f0ae94b6eb649fc995c94365ed2ac44 |
| Source note | uspto-grants-2011_09 |