反应详情

温度

70 °C

354 g of methoxypropyl acetate, 237 g (2 moles) of glycerol carbonate (Jeffsol GC from Huntsman; CAS RN: 931-40-8; molecular weight: 118.09) are introduced in succession, under nitrogen, into a three-necked flask equipped with a condenser and an addition funnel. The mixture is stirred at 230 revolutions per minute and heated to 70° C. Then 262.5 g (2.03 moles) of n-octylamine (CAS RN: 11-86-4; molecular weight: 129.25) are added to the reaction mixture in the course of 15 minutes. The reaction is strongly exothermic and the temperature of the reaction mixture reaches approximately 88° C.

1. customequipped with a condenser and an addition funnel
2. customreaches approximately 88° C.