1,3-Propanedithiol → 2-Methyl-2-dichloromethyl-1,3-dithiane

HRID 909120Notes

Reaction equation

HRID 909120 reaction equation
[Cl:1][CH:2]([Cl:6])[C:3]([CH3:5])=O.[CH2:7]([SH:11])[CH2:8][CH2:9][SH:10]>>[CH3:5][C:3]1([CH:2]([Cl:6])[Cl:1])[S:11][CH2:7][CH2:8][CH2:9][S:10]1

Participants

3

Reactant 2

HCID 80131,3-PropanedithiolHCID 105671,1-Dichloroacetone

Product 1

HCID 222387762-Methyl-2-dichloromethyl-1,3-dithiane

Procedure

In a further non-limiting embodiment, 1,1-dichloroacetone can be reacted with 1,3-propanedithiol to produce 2-methyl-2-dichloromethyl-1,3-dithiane, as shown below.

Sources & evidence

ORD record
ord-74061e9541c048a1a3c3c0465ef77af6
Source dataset
uspto-grants-2011_09
Patent number
US08017720B2

Reaction notes

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