1-(2-Bromoethyl)-2-chlorobenzene → HCID 53373727, compound

Participants

Reaction Steps

The title compound was prepared by a similar procedure described for step 7 of example 1 using 2-[(6-bromo-1,3-benzodioxol-5-yl)sulfanyl]-1H-imidazo[4,5-c]pyridin-4-amine and 1-(2-bromoethyl)-2-chloro-benzene. 1H NMR (DMSO-d6) δ; 7.69 (d, J=6.0 Hz, 1H), 7.36 (dd, J=8.0, 1.6 Hz, 1H), 7.32 (s, 1H), 7.23 (td, J=8.0, 1.6 Hz, 1H), 7.06 (td, J=7.2, 1.6 Hz, 1H), 6.72 (d, J=6.0 Hz, 1H), 6.52 (s, 1H), 6.38 (s, 2H), 6.06 (s, 2H), 4.45 (t, J=6.8 Hz, 2H), 3.09 (t, J=6.8 Hz, 2H); LC-MS [M+H]+ 502.99.

Provenance & Evidence