Hydrazine → HCID 178509224, Verbindung

HRID 909275Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 909275
[Br:1][C:2]1[CH:3]=[C:4]([C:9]#[N:10])[C:5](Cl)=[N:6][CH:7]=1.[NH2:11][NH2:12]>CCO>[Br:1][C:2]1[CH:3]=[C:4]2[C:9]([NH2:10])=[N:12][NH:11][C:5]2=[N:6][CH:7]=1

Komponenten

4

Edukt 2

HCID 9321HydrazineHCID 219482695-Bromo-2-chloronicotinonitrile

Produkt 1

HCID 178509224HCID 178509224, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Compound 3 (307 mg, 1.4 mmol) was dissolved in EtOH (10 mL) in a microwave tube, to which 5 equivalent of NH2NH2 was added, and the reaction mixture was put on Microwave irradiation for 10 min at 170° C. Evaporated the solvent to obtain the title compound 4 in quantative yield.

Aufarbeitung

  1. additionwas added
  2. customthe reaction mixture was put on Microwave irradiation for 10 min at 170° C
  3. customEvaporated the solvent

Quellen und Nachweise

ORD-Eintrag
ord-9ee545c92e134a59b87e2da1d90b5850
Quelldatensatz
uspto-grants-2011_09
Patentnummer
US08017781B2

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