HCID 58026771, compound → HCID 58026933, compound

Participants

Reaction Steps

8-Nitro-4-azabenzo[c]chromen-6-one (Reference Compound No. 1-3-(4), 368 mg, 1.52 mmol) was dissolved in methanol (10 mL), then 5% palladium on charcoal (37 mg) was added thereto, and then the reaction mixture was stirred under hydrogen atmosphere at room temperature for 4 days. After the mixture was filtered, the solvent was removed under reduced pressure. Chloroform was added to the obtained residue, and then filtered to give the titled reference compound (298 mg) as a yellow solid. (Yield 92%)

Provenance & Evidence