HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 909392Generated: October 26, 2026
5-Propylcyclohexane-1,3-dione → HCID 67410243, compound
https://huagongshe.com/reaction/909392
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 5-Propylcyclohexane-1,3-dione | HCID 2737224 | — |
| Reactant | 3-Aminocrotonitrile | HCID 5324720 | — |
| Reactant | 3-Bromo-4-(2-methoxy-ethylamino)-5-(morpholine-4-sulfonyl)-benzaldehyde | HCID 87389143 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67410243 | HCID 67410243 | — |
Reaction Steps
A mixture of the product of step d (61 mg), 3-aminocrotonitrile (12.3 mg) and 5-propylcyclohexane-1,3-dione (23.1 mg) in ethanol (5 ml) was stirred at 80° C. for 17 h. The reaction mixture was concentrated in vacuo and the residue was purified by preparative HPLC (Method B). Yield: 57 mg. MS-ESI: [M+H]+=607.3/609.3; HPLC: Rt=16.51 min. (diast. 1) Rt=16.83 min. (diast. 2) (method 1). Diast. ratio: 9:1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08017782B2 |
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| Source dataset | uspto-grants-2011_09 |
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| ORD ID | ord-b3007321c7f64c6fad9000e1d19d8875 |
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| Source note | uspto-grants-2011_09 |
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