HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenyl-1-cyclopentanol → Benzene, 1-cyclopenten-1-yl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenyl-1-cyclopentanol | HCID 139165 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzene, 1-cyclopenten-1-yl- | HCID 136652 | 85% |
Reaction Steps
The same experiment as in Example 3 was carried out, except for using 50 ml of THF instead of 50 ml of CPME. The resulting reaction mixture was analyzed by gas chromatography to confirm that the target 1-hydroxy-1-phenylcyclopentane and phenylcyclopentene were obtained in a yield of 85% in total.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08017813B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-27dd571849d64bbd90d425022f25ac80 |
| Source note | uspto-grants-2011_09 |