2-(2,4,6-Trimethylphenyl)propan-2-ol → 2-Isopropenyl-1,3,5-trimethylbenzene

HRID 909703노트

반응식

HRID 909703 반응식
[C:1]1([CH3:13])[CH:6]=[C:5]([CH3:7])[CH:4]=[C:3]([CH3:8])[C:2]=1[C:9](O)([CH3:11])[CH3:10]>C1COCC1>[CH3:11][C:9]([C:2]1[C:3]([CH3:8])=[CH:4][C:5]([CH3:7])=[CH:6][C:1]=1[CH3:13])=[CH2:10]

참가 물질

3

반응물 1

HCID 2930032-(2,4,6-Trimethylphenyl)propan-2-ol

생성물 1

HCID 5189862-Isopropenyl-1,3,5-trimethylbenzene수율 44.6%

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The same experiment as in Example 4 was carried out, except for using 50 ml of THF instead of 50 ml of CPME. The resulting reaction mixture was analyzed by gas chromatography to confirm that 2-mesityl-2-propanol and α-methyl-2,4,6-trimethylstyrene were obtained in a yield of 44.6% and 33.1%, respectively.

후처리

  1. customThe resulting reaction mixture

출처 및 근거

ORD 기록
ord-fa953b2c4d3a4654b5093e12452b056e
출처 데이터셋
uspto-grants-2011_09
특허 번호
US08017813B2

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