2-(Dimethylamino)ethanol → Bis(3,3'-(phenyl-dimethylaminoethoxyboryl)benzyl) ether

HRID 909819Notes

Reaction equation

HRID 909819 reaction equation
[C:1]1([B:7]([CH:9]([O:16][CH:17]([B:24]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[OH:25])[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[OH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:32][N:33]([CH3:37])[CH2:34][CH2:35]O>C(O)C>[C:1]1([B:7]([CH:9]([O:16][CH:17]([B:24]([C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=2)[O:25][CH2:35][CH2:34][N:33]([CH3:37])[CH3:32])[C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=2)[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[O:8][CH2:35][CH2:34][N:33]([CH3:37])[CH3:32])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 79022-(Dimethylamino)ethanolHCID 67392963Bis(3,3'-(phenylhydroxyboryl)benzyl) ether

Product 1

HCID 67392614Bis(3,3'-(phenyl-dimethylaminoethoxyboryl)benzyl) ether

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The entitled compound (60 mg) was obtained by allowing 95 mg of bis(4,4′-(phenylhydroxyboryl)benzyl) ether and 55 mg of N,N-dimethylethanolamine to act in 0.7 mL of ethanol at room temperature.

Sources & evidence

ORD record
ord-75e3a4f28b2142939ad6b4b492805966
Source dataset
uspto-grants-2011_09
Patent number
US08017809B2

Reaction notes

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