N-Methylaminoethanol → Bis(4,4'-(phenyl-N-methylaminoethoxyboryl)benzyl) ether

HRID 909820Notes

Reaction equation

HRID 909820 reaction equation
[C:1]1([B:7]([CH:9]([O:16][CH:17]([B:24]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[OH:25])[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[OH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:32][NH:33][CH:34](O)[CH3:35]>C(O)C>[C:1]1([B:7]([CH:9]([O:16][CH:17]([B:24]([C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=2)[O:25][CH2:35][CH2:34][NH:33][CH3:32])[C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=2)[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[O:8][CH2:35][CH2:34][NH:33][CH3:32])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 5247031N-MethylaminoethanolHCID 67392963Bis(3,3'-(phenylhydroxyboryl)benzyl) ether

Product 1

HCID 67392160Bis(4,4'-(phenyl-N-methylaminoethoxyboryl)benzyl) ether

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The entitled compound (8 mg) was obtained by allowing 20 mg of bis(4,4′-(phenylhydroxyboryl)benzyl) ether and 7.3 mg of N-methylaminoethanol to act in 0.7 mL of ethanol at room temperature.

Sources & evidence

ORD record
ord-5bfac1c8efaa44778de381632cd07029
Source dataset
uspto-grants-2011_09
Patent number
US08017809B2

Reaction notes

Loading…