2-(Methylamino)ethanol → HCID 67391993, compound

HRID 909825Notes

Reaction equation

HRID 909825 reaction equation
[CH3:1][NH:2][CH2:3][CH2:4][OH:5].[Cl:6][C:7]1[CH:8]=[C:9]([B:14]([CH:16]([O:23][CH:24]([B:31]([C:33]2[CH:38]=[CH:37][C:36]([CH3:39])=[C:35]([Cl:40])[CH:34]=2)[OH:32])[C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)O)[CH:10]=[CH:11][C:12]=1[CH3:13]>C(O)C>[Cl:6][C:7]1[CH:8]=[C:9]([B:14]([CH:16]([O:23][CH:24]([B:31]([C:33]2[CH:38]=[CH:37][C:36]([CH3:39])=[C:35]([Cl:40])[CH:34]=2)[O:32][CH2:4][CH2:3][NH:2][CH3:1])[C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[O:5][CH2:4][CH2:3][NH:2][CH3:1])[CH:10]=[CH:11][C:12]=1[CH3:13]

Participants

4

Reactant 2

HCID 80162-(Methylamino)ethanolHCID 67392188HCID 67392188, compound

Product 1

HCID 67391993HCID 67391993, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The entitled compound (31 mg) was obtained by allowing 32 mg of N-methylethanolamine to act on 99 mg of bis(4,4′-(3-chloro-4-methylphenyl-hydroxyboryl)benzyl) ether in 0.5 mL of ethanol.

Sources & evidence

ORD record
ord-32a97a86d7a741d5b6bc59dcc323c3b2
Source dataset
uspto-grants-2011_09
Patent number
US08017809B2

Reaction notes

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