DL-Phenylalaninol → HCID 67392364, compound

HRID 909839Notes

Reaction equation

HRID 909839 reaction equation
[C:1]1([B:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[O:15][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=2[B:22]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[OH:23])[OH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH2:30][CH:31]([CH2:34][C:35]1[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1)[CH2:32]O>C(#N)C>[C:1]1([B:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[O:15][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=2[B:22]([C:24]2[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=2)[O:23][CH2:32][CH:31]([CH2:34][C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[NH2:30])[O:8][CH2:32][CH:31]([CH2:34][C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[NH2:30])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 76652DL-PhenylalaninolHCID 67392250HCID 67392250, compound

Product 1

HCID 67392364HCID 67392364, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

The entitled compound (73 mg) was obtained by allowing 77 mg of bis(4,4′-(phenylhydroxyboryl)phenyl) ether and 75 mg of 2-amino-3-phenylpropanol to act in 1 mL of acetonitrile.

Sources & evidence

ORD record
ord-bbac92785cd5479f95cba4a9d60c0b1b
Source dataset
uspto-grants-2011_09
Patent number
US08017809B2

Reaction notes

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