HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 909903Generated: October 30, 2026
Trifluoroacetic acid → HCID 59290395, compound
https://huagongshe.com/reaction/909903
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | tert-butyl 3-(3-(1-methyl-1H-tetrazol-5-yl)phenethoxy)propanoate | HCID 67076290 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59290395 | HCID 59290395 | — |
Reaction Steps
A mixture of tert-butyl 3-(3-(1-methyl-1H-tetrazol-5-yl)phenethoxy)propanoate [Example 7, Step iii)] (135 mg), DCM (4 mL) and TFA (4 mL) was stirred at 25° C. for 30 min and concentrated under vacuum to afford the subtitled compound as a gum. 1H NMR (400 MHz, CDCl3) δ 7.72 (s, 1H), 7.53-7.41 (m, 3H), 4.18 (s, 3H), 3.78-3.72 (m, 4H), 2.96 (t, J=5.9 Hz, 2H), 2.59 (t, J=5.9 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08017602B2 |
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| Source dataset | uspto-grants-2011_09 |
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| ORD ID | ord-aed06114bcee4e438fe0d8733532afca |
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| Source note | uspto-grants-2011_09 |
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