HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzamide → {4-Bromo-2-[2-(4-chlorophenyl)oxazol-4-yl]phenoxy}acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzamide | HCID 12084 | — |
| Reactant | [4-Bromo-2-(2-bromoacetyl)phenoxy]acetic acid ethyl ester | HCID 57658801 | — |
| Product | {4-Bromo-2-[2-(4-chlorophenyl)oxazol-4-yl]phenoxy}acetic acid | HCID 57658748 | — |
Reaction Steps
Title compound was prepared from [4-bromo-2-(2-bromoacetyl)phenoxy]acetic acid ethyl ester and 4-chlorobenzamide according to GP5 and GP3: LC/MS (an10p8) Rt 2.90 min, m/z 407.7 [M+H]+; 1H NMR (CDCl3): δ 4.89 (s, 2H), 7.09 (d, 1H), 7.48 (d, 1H), 7.64 (d, 2H), 8.08 (d, 2H), 8.20 (s, 1H), 8.89 (s, 1H), 13.2 (br s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022063B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-9d8ba2ce14b241ffb696259897f92bf3 |
| Source note | uspto-grants-2011_09 |