4-(Bromomethyl)pyridine → HCID 57658785, compound

HRID 910057Notes

Reaction equation

HRID 910057 reaction equation
Br[CH2:2][C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1.C([O:11][C:12](=[O:30])[CH2:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([Br:21])=[CH:17][C:16]=1/[CH:22]=[C:23]1/[C:24](=[O:29])[NH:25][C:26](=[O:28])[S:27]/1)C>>[Br:21][C:18]1[CH:19]=[CH:20][C:15]([O:14][CH2:13][C:12]([OH:30])=[O:11])=[C:16]([CH2:22][CH:23]2[S:27][C:26](=[O:28])[N:25]([CH2:2][C:3]3[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=3)[C:24]2=[O:29])[CH:17]=1

Participants

3

Reactant 2

HCID 6427994-(Bromomethyl)pyridineHCID 16634246HCID 16634246, compound

Product 1

HCID 57658785HCID 57658785, compound

Procedure

Prepared from 4-bromomethylpyridine and 4-bromo-2-[2,4-dioxothiazolidin-(5Z)-ylidenemethyl]phenoxyacetic acid ethyl ester according to GP13, GP14 and GP16: LC/MS (an10p8): Rt 2.1 min, m/z 451 [M+H]+.

Sources & evidence

ORD record
ord-4968043ba37c478981d74d4f20306224
Source dataset
uspto-grants-2011_09
Patent number
US08022063B2

Reaction notes

Loading…