HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-5-ethoxy-4-hydroxybenzaldehyde → 2-(2-Bromo-6-ethoxy-4-formyl-phenoxymethyl)-furan-3-carboxylic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-5-ethoxy-4-hydroxybenzaldehyde | HCID 612496 | — |
| Reactant | Methyl 2-(Bromomethyl)-3-Furoate | HCID 2736827 | — |
| Product | 2-(2-Bromo-6-ethoxy-4-formyl-phenoxymethyl)-furan-3-carboxylic acid methyl ester | HCID 86624409 | — |
Reaction Steps
Alkylation of 3-bromo-5-ethoxy-4-hydroxy benzaldehyde (123 mg) with 2-bromomethyl-furan-3-carboxylic acid methyl ester (109 mg) was performed according to the method described in example 1a. Yield: 191 mg. MS-ESI: [M+H]+=383/385
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022218B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-343dc2bb77fa45b8846f2709dd2737e3 |
| Source note | uspto-grants-2011_09 |