HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 5-(chloromethyl)-1,3-dimethyl-1H-pyrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (1,3-dimethyl-1H-pyrazol-5-yl)methanol | HCID 2776363 | — |
| Product | 5-(chloromethyl)-1,3-dimethyl-1H-pyrazole | HCID 4961270 | — |
Reaction Steps
The title compound was prepared analogously to example 48b starting from (2,5-dimethyl-2H-pyrazol-3-yl)-methanol (778 mg) and thionyl chloride (2.35 ml). Yield: 900 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022218B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-7d354bc6ec1147e591a1732b2e30a972 |
| Source note | uspto-grants-2011_09 |