Diethyl disulfide → HCID 67391976, compound

HRID 910859Notes

Reaction equation

[Cl:1][C:2]1[CH:9]=[CH:8][C:7]([S:10][CH3:11])=[CH:6][C:3]=1[C:4]#[N:5].[CH2:12](SSCC)C>>[Cl:1][C:2]1[CH:9]=[CH:8][C:7]([S:10][CH2:11][CH3:12])=[CH:6][C:3]=1[C:4]#[N:5]

Participants

Reactant 2

HCID 8077Diethyl disulfide

HCID 69225444HCID 69225444, compound

Product 1

HCID 67391976HCID 67391976, compound

Procedure

The subtitle compound was prepared by the method of example 5 step iv) using the product from step i) and diethyldisulphide. Yield 2.50 g.

Sources & evidence

ORD record: ord-7aa2665ebcc049fba0d6b795ac53f038
Source dataset: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08022248B2

Reaction notes

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