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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 910863Generated: October 29, 2026

HCID 67391626, compound → HCID 67391135, compound

https://huagongshe.com/reaction/910863

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67391626HCID 67391626—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
ProductHCID 67391135HCID 67391135—

Reaction Steps

A mixture of the product from step (ii) (0.2 g) and Pd(OH)2/C (0.04 g) in ethanol (4 ml) was hydrogenated at 1 Bar for 5 h then filtered. The filtrate was evaporated under reduced pressure and the residue purified by chromatography on silica eluting with 20% ethylacetate/isohexane, yield 0.13 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08022248B2
Source datasetuspto-grants-2011_09
ORD IDord-82ae4b0d02574831a831dc9620d6499c
Source noteuspto-grants-2011_09