HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67391626, compound → HCID 67391135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67391626 | HCID 67391626 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67391135 | HCID 67391135 | — |
Reaction Steps
A mixture of the product from step (ii) (0.2 g) and Pd(OH)2/C (0.04 g) in ethanol (4 ml) was hydrogenated at 1 Bar for 5 h then filtered. The filtrate was evaporated under reduced pressure and the residue purified by chromatography on silica eluting with 20% ethylacetate/isohexane, yield 0.13 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022248B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-82ae4b0d02574831a831dc9620d6499c |
| Source note | uspto-grants-2011_09 |