Benzoyl isothiocyanate → HCID 86634745, compound

Participants

Reaction Steps

Benzoyl isothiocyanate (1.63 g, 10.0 mmol) is added to a solution of 5-bromo-4-(2,6-difluorophenoxy)pyridin-2-amine (3.01 g, 10 mmol) in dichloromethane (20 mL) at 0° C. The reaction mixture is warmed to room temperature and stirred for one hour. The reaction mixture is diluted with hexanes and filtered to afford N-(5-bromo-4-(2,6-difluorophenoxy)pyridin-2-ylcarbamothioyl)benzamide.

Provenance & Evidence