HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinemethanamine → 4-(Aminomethyl)-N-(2-pyridinylmethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Reactant | 4-(((tert-Butoxycarbonyl)amino)methyl)benzoic acid | HCID 853605 | — |
| Product | 4-(Aminomethyl)-N-(2-pyridinylmethyl)benzamide | HCID 16790594 | 106% |
Reaction Steps
Use the General Procedure 6-2, using 2-(aminomethyl)pyridine (181 mg, 0.172 mL, 1.67 mmol) and 4-(tert-butoxycarbonylamino-methyl)-benzoic acid (420 mg, 1.67 mmol) to give the title compound as a solid (427 mg, 100%). MS (ES+) m/z: 242 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022062B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-bb8ed99c5a954852818bea75c38c62f7 |
| Source note | uspto-grants-2011_09 |