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HRID911467

反应详情

EQUATION

反应方程式

HRID 911467 的结构方程式

REACTANTS

反应物

2
结构：Fc1cc(CBr)ccc1Br
HCID11666176

4-Bromo-3-fluorobenzyl bromide

C7H5Br2F

结构：CN(C)C(=O)Sc1c(Cl)ccc2c1CCN(C(=O)OC(C)(C)C)CC2
HCID57655979

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCc2ccc(Cl)c(SCc3ccc(Br)c(F)c3)c2CC1
HCID57656268

未命名化合物

PROCEDURE

实验过程

Use a method similar to the Preparation 177, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 1-bromo-4-bromomethyl-2-fluorobenzene, to give the title compound as a white solid.

WORKUP

后处理

  1. customsimilar to the Preparation 177