HRID911494

反应详情

EQUATION

反应方程式

HRID 911494 的结构方程式

PROCEDURE

实验过程

Use a method similar to the Example 366 to react 6-(5-bromo-pyridin-2-ylmethylthio)-3-tert-butoxycarbonyl-7-chloro-2,3,4,5-tetrahydro-1H-benzo[d]azepine with cyclohexylmethylzinc bromide. Use a method similar to the General Procedure 1-5, basic workup, and a method similar to the General Procedure 2-2 to give the title compound as a white solid. MS (APCI+) m/z: 401 (M+H)+.