HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-tert-butoxycarbonyl-7-chloro-6-dimethylaminocarbonylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine → HCID 66706735, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-tert-butoxycarbonyl-7-chloro-6-dimethylaminocarbonylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine | HCID 57655979 | — |
| Reactant | HCID 57656381 | HCID 57656381 | — |
| Product | HCID 66706735 | HCID 66706735 | — |
Reaction Steps
Use a method similar to the Preparation 177 to react 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 1-bromomethyl-4-(2,2-dimethylpropoxy)-benzene. Use a method similar to the General Procedure 1-4 to give the title compound as a white solid. MS (ES+) m/z: 390 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022062B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-706795f5e3ad4d8eacaf4da07fdf27fb |
| Source note | uspto-grants-2011_09 |