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HRID911524

反应详情

EQUATION

反应方程式

HRID 911524 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)c1ccccc1CBr
HCID18922474

1-(Bromomethyl)-2-(methanesulfonyl)benzene

C8H9BrO2S

结构：CN(C)C(=O)Sc1c(Cl)ccc2c1CCN(C(=O)OC(C)(C)C)CC2
HCID57655979

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)(=O)c1ccccc1CSc1c(Cl)ccc2c1CCNCC2.Cl
HCID66706654

未命名化合物

PROCEDURE

实验过程

Use a method similar to the Preparation 177, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 1-bromomethyl-2-methanesulfonyl-benzene to give, after deprotection by the General Procedure 1-4, the title compound and as a white solid. MS (APCI+) m/z: 382 (M+H)+.

WORKUP

后处理

  1. customsimilar to the Preparation 177
  2. customto give