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HRID911526

反应详情

EQUATION

反应方程式

HRID 911526 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C(=O)Sc1c(Cl)ccc2c1CCN(C(=O)OC(C)(C)C)CC2
HCID57655979

未命名化合物

结构：CC(C)(C)CC(=O)c1ccc(CBr)cc1
HCID57656172

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)CC(=O)c1ccc(CSc2c(Cl)ccc3c2CCNCC3)cc1.Cl
HCID66706869

未命名化合物

PROCEDURE

实验过程

Use a method similar to the Example 428 to react 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine with 1-(4-bromomethylphenyl)-3,3-dimethylbutan-1-one. Use a method similar to the General Procedure 1-4, basic workup, and a method similar to the General Procedure 2-2 to give the title compound as a white solid. MS (APCI+) m/z: 402 (M+H)+.