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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 911536Generated: October 30, 2026

Methyl bromoacetate → HCID 66707067, compound

https://huagongshe.com/reaction/911536

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl bromoacetateHCID 60984—
Reactant3-tert-butoxycarbonyl-7-chloro-6-dimethylaminocarbonylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepineHCID 57655979—
ProductHCID 66707067HCID 66707067—

Reaction Steps

Use a method similar to the Example 347, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and methyl bromoacetate to give 3-tert-butoxycarbonyl-7-chloro-6-methoxycarbonylmethylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08022062B2
Source datasetuspto-grants-2011_09
ORD IDord-ad8135af08c04e8393fbf60fa5f50985
Source noteuspto-grants-2011_09