Npc164516 → 8-Methyl-3-(trimethylstannyl)-8-azabicyclo[3.2.1]oct-2-ene

HRID 911990Notes

Reaction equation

HRID 911990 reaction equation
[CH3:1][N:2]1[CH:7]2[CH2:8][CH2:9][CH:3]1[CH2:4][C:5](=O)[CH2:6]2.C(N1CC=[C:18]([Sn:21](C)([CH3:23])[CH3:22])CC1)(C)(C)C>>[CH3:1][N:2]1[CH:7]2[CH2:8][CH2:9][CH:3]1[CH:4]=[C:5]([Sn:21]([CH3:23])([CH3:22])[CH3:18])[CH2:6]2

Participants

3

Reactant 2

HCID 79038Npc164516HCID 226481771-Tert-butyl-4-(trimethylstannyl)-1,2,3,6-tetrahydropyridine

Product 1

HCID 235329158-Methyl-3-(trimethylstannyl)-8-azabicyclo[3.2.1]oct-2-ene

Procedure

The compound was prepared from 8-methyl-8-azabicyclo[3.2.1]octan-3-one as described above for 1-tert-Butyl-1,2,3,6-tetrahydro-4-(trimethylstannyl)pyridine.

Sources & evidence

ORD record
ord-c6c64934260a4dc0b0ce6eafeadd34ab
Source dataset
uspto-grants-2011_09
Patent number
US08022206B2

Reaction notes

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