HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodo-4-nitrobenzene → N-(2-Morpholinoethyl)-4-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodo-4-nitrobenzene | HCID 12495 | — |
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Product | N-(2-Morpholinoethyl)-4-nitroaniline | HCID 21975017 | — |
Reaction Steps
Using 1-iodo-4-nitro-benzene (498 mg) instead of 1-bromo-3-nitro-benzene, and 2-morpholin-4-yl-ethylamine (315 μl) instead of morpholine, in the same manner as Step A in Example 1-D-105, the desired compound was obtained (301.1 mg, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08022205B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-d37bca708cae478da5645a8ea4e5474c |
| Source note | uspto-grants-2011_09 |