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Acetic Anhydride → N-(3,5-dimethoxyphenyl)acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | Hexane | HCID 8058 | — |
| 反応物 | 3,5-Dimethoxyaniline | HCID 66301 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N-(3,5-dimethoxyphenyl)acetamide | HCID 702039 | — |
反応手順
To a solution of 3,5-dimethoxy-phenylamine (22.0 g, 143.6 mmol) in toluene (100 mL), is added slowly Ac2O (14 mL) at room temperature. After stirring 30 minutes, hexane (50 mL) is added with stirring at room temperature. The resulting solid is filtered and washed with hexane (50 mL) to offer designed product as a white solid 14.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08026243B2 |
| 出典データセット | uspto-grants-2011_09 |
| ORD ID | ord-64bcb4283a7945a9bd9298d6aa0737d0 |
| 出典メモ | uspto-grants-2011_09 |