HRID912649

反应详情

EQUATION

反应方程式

HRID 912649 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in accordance with the general method described in Example 1(b) using N-(pyridin-3-ylmethyl)thiourea (Beaudegnies, R., Wendeborm, S., Heterocycles, 2003, 11, 2417-2424) (1.19 g, 7.12 mmol) and ethyl cyanoacetate (0.97 g, 8.54 mmol), giving the title compound (1.38 g, 83%) as a solid.

WORKUP

后处理

  1. customThe title compound was prepared in accordance with the general method