Ethyl [(phenoxycarbonyl)oxy]acetate → HCID 67415750, compound

HRID 912736Notes

Reaction equation

HRID 912736 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:9][CH:10]2[CH2:15][CH2:14][NH:13][CH2:12][CH2:11]2)=[CH:4][CH:3]=1.C1([O:22][C:23]([O:25][CH2:26][C:27]([O:29][CH2:30][CH3:31])=[O:28])=O)C=CC=CC=1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:9][CH:10]2[CH2:11][CH2:12][N:13]([C:23]([O:25][CH2:26][C:27]([O:29][CH2:30][CH3:31])=[O:28])=[O:22])[CH2:14][CH2:15]2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 12094709Ethyl [(phenoxycarbonyl)oxy]acetateHCID 249023594-[(4-Bromophenoxy)methyl]piperidine

Product 1

HCID 67415750HCID 67415750, compound

Procedure

The procedure described in Example 4.3. is repeated. Starting from 1.6 g (5.9 mmol) of 4-{[(4-bromophenyl)oxy]methyl}piperidine, prepared in Step 5.2., and from 1.32 g (5.9 mmol) of ethyl {[(phenyloxy)carbonyl]oxy}acetate, prepared in accordance with Example 1.1., gives the product in oil form.

Workup

  1. customprepared in Step 5.2
  2. custom, gives the product in oil form

Sources & evidence

ORD record
ord-030c9c0b3f6b410aa97cd234649613d0
Source dataset
uspto-grants-2011_09
Patent number
US08026258B2

Reaction notes

Loading…