HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5,6-Trichloro-1H-benzimidazole → HCID 57835131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5,6-Trichloro-1H-benzimidazole | HCID 286009 | — |
| Reactant | 1-[3-(Trifluoromethyl)pyridin-2-yl]piperazine | HCID 2777786 | — |
| Product | HCID 57835131 | HCID 57835131 | — |
Reaction Steps
The benzoimidazole from step (b) above (0.110 g, 0.5 mmol) and 1-(3-trifluoromethylpyridin-2-yl)piperazine (0.231 g, 1 mmol, Maybridge) reacted under the conditions Example 3c to give the title compound as a white amorphous solid. MS (ESI, pos. ion) m/z: 416 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026241B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-341d222773de4d589f7be56a6efbefe0 |
| Source note | uspto-grants-2011_09 |